MARC details
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10069nam a2200733 i 4500 |
| 001 - CONTROL NUMBER |
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| control field |
EBC1747024 |
| 003 - CONTROL NUMBER IDENTIFIER |
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| control field |
MiAaPQ |
| 006 - FIXED-LENGTH DATA ELEMENTS--ADDITIONAL MATERIAL CHARACTERISTICS--GENERAL INFORMATION |
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m o d | |
| 007 - PHYSICAL DESCRIPTION FIXED FIELD--GENERAL INFORMATION |
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cr cnu|||||||| |
| 008 - FIXED-LENGTH DATA ELEMENTS--GENERAL INFORMATION |
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| fixed length control field |
141014s2014 nyua foab 001 0 eng d |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| International Standard Book Number |
9781606504376 |
| Qualifying information |
electronic |
| 020 ## - INTERNATIONAL STANDARD BOOK NUMBER |
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| Cancelled/invalid ISBN |
9781606504352 |
| Qualifying information |
print |
| 024 7# - OTHER STANDARD IDENTIFIER |
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| Canceled/invalid standard number or code |
10.5643/9781606504376 |
| Source of number or code |
doi |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(OCoLC)892991224 |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(CaBNvSL)swl00404108 |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(MiAaPQ)EBC1747024 |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(Au-PeEL)EBL1747024 |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(CaPaEBR)ebr10951845 |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(CaONFJC)MIL629602 |
| 035 ## - SYSTEM CONTROL NUMBER |
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| System control number |
(OCoLC)884647645 |
| 040 ## - CATALOGING SOURCE |
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| Original cataloging agency |
MiAaPQ |
| Language of cataloging |
eng |
| Description conventions |
rda |
| -- |
pn |
| Transcribing agency |
MiAaPQ |
| Modifying agency |
MiAaPQ |
| 050 #4 - LIBRARY OF CONGRESS CALL NUMBER |
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| Classification number |
QD96.A8 |
| Item number |
S262 2014 |
| 082 0# - DEWEY DECIMAL CLASSIFICATION NUMBER |
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| Classification number |
543.0858 |
| Edition number |
23 |
| 100 1# - MAIN ENTRY--PERSONAL NAME |
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| Personal name |
Sanz-Medel, Alfredo., |
| Relator term |
author. |
| 245 10 - TITLE STATEMENT |
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| Title |
Atomic absorption spectrometry : |
| Remainder of title |
an introduction / |
| Statement of responsibility, etc |
Alfredo Sanz-Medel and Rosario Pereiro. |
| 250 ## - EDITION STATEMENT |
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| Edition statement |
Second edition. |
| 264 #1 - |
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| -- |
New York, [New York] (222 East 46th Street, New York, NY 10017) : |
| -- |
Momentum Press, |
| -- |
2014. |
| 300 ## - PHYSICAL DESCRIPTION |
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| Extent |
1 online resource (xiii, 190 pages) : |
| Other physical details |
illustrations. |
| 336 ## - |
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| -- |
text |
| -- |
rdacontent |
| 337 ## - |
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| -- |
computer |
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rdamedia |
| 338 ## - |
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| -- |
online resource |
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rdacarrier |
| 504 ## - BIBLIOGRAPHY, ETC. NOTE |
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| Bibliography, etc |
Includes bibliographical references (pages 179-184) and index. |
| 505 0# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
1. An introduction to analytical atomic spectrometry -- 1.1 Basic interactions of electromagnetic radiation with atoms for chemical analysis -- 1.2 Atomic line spectra and their origin -- 1.3 Atomic line characteristics -- 1.4 Atomic line spectral width -- 1.4.1 Natural broadening of lines -- 1.4.2 Doppler broadening -- 1.4.3 Lorentz broadening -- 1.4.4 Self-absorption effects -- 1.4.5 Other broadening processes -- 1.5 A comparative overview of analytical atomic spectrometric techniques -- 1.5.1 Dissolved sample analysis techniques -- 1.5.2 Direct solid analysis techniques -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
2. Theory and basic concepts in atomic absorption spectrometry -- 2.1 General introduction -- 2.2 The basic atomic absorption spectrometry experiment -- 2.3 The absorption coefficient concept -- 2.4 Quantitative analysis by atomic absorption spectrometry -- 2.5 Interferences in flame analytical atomic spectrometry techniques -- 2.5.1 Spectral interferences -- 2.5.2 Physical (transport) interferences -- 2.5.3 Chemical interferences -- 2.5.4 Ionization interferences -- 2.5.5 Temperature variations in the atomizer -- 2.5.6 Light scattering and unspecific absorptions -- 2.5.7 Quenching of the fluorescence -- 2.6 Analytical performance characteristics of AAS -- 2.6.1 Sensitivity and detection limits -- 2.6.2 Selectivity of the three flame-based techniques -- 2.6.3 Accuracy and precision -- 2.6.4 Analytical linear range -- 2.6.5 Versatility and sample throughput -- 2.6.7 Robustness and availability of well-proven methodologies -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
3. Basic components of atomic absorption spectrometric instruments -- 3.1 Introduction: single-beam and double-beam instruments -- 3.2 Primary radiation sources -- 3.2.1 Hollow cathode lamps -- 3.2.1.1 Details of the components of a HCL -- 3.2.1.2 HCL operation -- 3.2.1.3 Multi-element HCLs -- 3.2.2 Electrodeless discharge lamps -- 3.2.3 Boosted discharge lamps -- 3.2.4 Diode lasers -- 3.2.5 Continuous sources -- 3.3 Atomizers: a general view -- 3.4 Wavelength selectors -- 3.5 Detectors -- 3.6 Background correctors -- 3.6.1 Deuterium background corrector -- 3.6.2 Zeeman correction -- 3.6.3 Smith-Hieftje correction -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
4. Flame atomic absorption spectrometry -- 4.1 Introduction -- 4.2 The atomizer unit in flame atomic absorption spectrometry -- 4.2.1 Nebulizer, nebulization chamber, and burner -- 4.2.2 Flame -- 4.2.3 Special sampling techniques -- 4.3 Flame atomic absorption instrumentation -- 4.3.1 Flame atomic absorption spectrometers -- 4.3.2 Accessories -- 4.3.2.1 Autosamplers -- 4.3.2.2 Atom concentrator tube or slotted tube atom trap -- 4.3.2.3 High-solid analyzer -- 4.3.2.4 Flame microsampler -- 4.3.2.5 Automatic burner rotation -- 4.4 Analytical performance characteristics and interferences -- 4.4.1 Spectral interferences -- 4.4.2 Nonspectral interferences -- 4.4.3 Calibration in flame atomic absorption spectrometry -- 4.4.4 Analytical figures of merit -- 4.4.5 Use of organic solvents -- 4.5 Applications and example case studies -- 4.5.1 Determination of calcium in milk -- 4.5.2 Determination of molybdenum in fertilizers -- 4.5.3 Determination of lead in gasoline -- 4.5.4 Determination of boron, phosphorus, and sulfur by high-resolution continuum source FAAS for plant analysis -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
5. Electrothermal atomic absorption spectrometry -- 5.1 Introduction -- 5.2 The electrothermal atomizer -- 5.2.1 The atomization tube -- 5.2.2 Side-heated atomizers -- 5.3 Basic steps in analysis by electrothermal atomic absorption spectrometry: the temperature program -- 5.4 Instrumentation -- 5.4.1 Sample-introduction system -- 5.4.2 Instrumental background correction -- 5.4.3 Data acquisition and treatment -- 5.5 Interferences -- 5.5.1 Spectral interferences -- 5.5.2 Nonspectral interferences -- 5.6 Chemical modifiers -- 5.7 Atomization from solids and slurries -- 5.8 Analytical performance characteristics of electrothermal atomic absorption spectrometric methods -- 5.9 Applications and example case studies -- 5.9.1 Determination of lead in human urine and blood -- 5.9.2 Determination of selenium in human milk -- 5.9.3 Determination of sulfur in coal and ash slurry -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
6. Hydride generation and cold-vapor atomic absorption spectrometry -- 6.1 Introduction -- 6.2 Volatile hydride generation by tetrahydroborate (III) in aqueous media -- 6.2.1 Mechanisms of hydride formation -- 6.2.2 Basic instrumentation -- 6.2.3 Limits of detection -- 6.2.4 Selectivity: sources of interferences -- 6.3 Electrochemical generation of volatile hydrides -- 6.4 Cold-vapor generation -- 6.4.1 Mercury -- 6.4.2 Cadmium -- 6.5 Trapping/preconcentration of volatilized analytes -- 6.6 Applications and example case studies -- 6.6.1 Determination of arsenic in waters -- 6.6.2 Determination of mercury and methylmercury in hair -- 6.6.3 Determination of selenium in bean and soil samples using hydride generation, electrothermal atomic absorption spectrometry -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
7. Flow analysis and atomic absorption spectrometry -- 7.1 Introduction -- 7.2 Flow injection analysis and atomic absorption spectrometry -- 7.3 Basic instrument components: sample introduction unit, propulsion system, and connecting tubes -- 7.3.1 Sample introduction unit -- 7.3.2 Propulsion system -- 7.3.3 Connecting tubes -- 7.4 Simple common manifolds: dilution, reagent addition, and calibration -- 7.5 Solid-liquid separation and preconcentration -- 7.5.1 Sorption -- 7.5.2 Precipitation and coprecipitation -- 7.6 Gas-phase formation strategies -- 7.6.1 Flow systems for the formation of volatile derivatives of the analyte(s) -- 7.6.2 Approaches for preconcentration in the gas phase -- 7.7 Miniaturized preconcentration methods based on liquid-liquid extraction -- 7.8 Sample digestion -- 7.8.1 Online photo-oxidation flow systems -- 7.8.2 Online microwave-assisted digestion -- 7.9 Chromatographic separations coupled online to atomic absorption spectrometry -- 7.10 Applications and example case studies -- 7.10.1 Online aluminium preconcentration and its application to the determination of the metal in dialysis concentrates -- 7.10.2 Indirect atomic absorption spectrometric determination of iodine in milk products -- 7.10.3 High-performance liquid chromatography, microwave digestion, hydride generation, AAS for inorganic and organic arsenic speciation in fish tissue -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
8. Emerging fields of applications, chemometrics, quality-control and troubleshooting -- 8.1 Emerging fields of atomic absorption spectrometry applications -- 8.2 Basic chemometric techniques in AAS -- 8.3 Quality-control guidelines and troubleshooting -- 8.3.1 Flame AAS -- 8.3.1.1 Light system -- 8.3.1.2 Nebulizer and burner system -- 8.3.1.3 System cleanliness -- 8.3.2 Electrothermal AAS -- 8.3.2.1 Autosampler -- 8.3.2.2 Furnace workhead -- 8.3.2.3 Background correction -- |
| 505 8# - FORMATTED CONTENTS NOTE |
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| Formatted contents note |
Appendix A. Buyer's guide -- Appendix B. Glossary of terms -- Appendix C. Standards -- References -- Index. |
| 506 ## - RESTRICTIONS ON ACCESS NOTE |
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| Terms governing access |
Restricted to libraries which purchase an unrestricted PDF download via an IP. |
| 520 3# - SUMMARY, ETC. |
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| Summary, etc |
We have restricted the scope of this tutorial book to the study of fundamentals and practical use of such popular and efficient atomic absorption techniques. An up-to-date account of AAS fundamentals, instrumentation, special techniques, and elemental analysis applications is provided here. To do so, the atomic absorption experiment and the photophysical law governing such photon absorption processes are revised first. Then, the main components or units, that, when adequately assembled, constitute an AAS instrument, are described in detail to set the foundations of modern spectrometers for AAS measurements. |
| 588 ## - |
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| -- |
Title from PDF title page (viewed on October 14, 2014). |
| 590 ## - LOCAL NOTE (RLIN) |
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| Local note |
Electronic reproduction. Ann Arbor, MI : ProQuest, 2015. Available via World Wide Web. Access may be limited to ProQuest affiliated libraries. |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name as entry element |
Atomic absorption spectroscopy. |
| 650 #0 - SUBJECT ADDED ENTRY--TOPICAL TERM |
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| Topical term or geographic name as entry element |
Flow injection analysis. |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
atomic absorption spectrometry (AAS) |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
characterization of nanoparticles |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
chemometrics |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
chromatographic separations |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
cold vapor generation |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
electrothermal (ET) atomization |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
elemental analysis |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
flow injection analysis (FIA) |
| 653 ## - INDEX TERM--UNCONTROLLED |
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| Uncontrolled term |
hydride vapor generation |
| 655 #4 - INDEX TERM--GENRE/FORM |
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| Genre/form data or focus term |
Electronic books. |
| 700 1# - ADDED ENTRY--PERSONAL NAME |
|---|
| Personal name |
Pereiro, Rosario., |
| Relator term |
author. |
| 776 08 - ADDITIONAL PHYSICAL FORM ENTRY |
|---|
| Display text |
Print version: |
| International Standard Book Number |
9781606504352 |
| 797 2# - LOCAL ADDED ENTRY--CORPORATE NAME (RLIN) |
|---|
| Corporate name or jurisdiction name as entry element |
ProQuest (Firm) |
| 856 40 - ELECTRONIC LOCATION AND ACCESS |
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| Uniform Resource Identifier |
<a href="https://ebookcentral.proquest.com/lib/bcsl-ebooks/detail.action?docID=1747024">https://ebookcentral.proquest.com/lib/bcsl-ebooks/detail.action?docID=1747024</a> |
| Public note |
Click to View |